Materials science and engineering of carbon characterization /
Materials Science and Engineering of Carbon: Characterization discusses 12 characterization techniques, focusing on their application to carbon materials, including X-ray diffraction, X-ray small-angle scattering, transmission electron microscopy, Raman spectroscopy, scanning electron microscopy, im...
| Other Authors: | Inagaki, Michio,, Kang, Feiyu,, ScienceDirect (Online service) |
|---|---|
| Format: | eBook |
| Language: | English |
| Published: |
Kidlington, Oxford, UK :
Butterworth-Heinemann is an imprint of Elsevier,
2016.
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| Physical Description: |
1 online resource. |
| Subjects: |
Table of Contents:
- Front Cover; Materials Science and Engineering of Carbon: Characterization; Materials Science and Engineering of Carbon: Characterization ; Copyright; Contents; Companion Web Site; List of Contributors; Preface; Acknowledgments; 1
- Introduction; 1.1 CARBON MATERIALS; 1.2 CHARACTERIZATION OF CARBON MATERIALS; 1.3 STRUCTURE OF THE PRESENT BOOK; REFERENCES; 2
- X-ray Powder Diffraction; 2.1 INTRODUCTION; 2.2 X-RAY DIFFRACTION PATTERN OF CARBON MATERIALS; 2.3 PARAMETERS DETERMINED BY X-RAY DIFFRACTION; 2.4 INSTRUMENTATION; 2.5 SPECIFICATIONS FOR MEASUREMENT.
- 2.5.1 PREPARATION OF SAMPLE FOR X-RAY MEASUREMENTS2.5.2 MEASUREMENT AND INTENSITY CORRECTION OF DIFFRACTION PROFILES; 2.5.3 CORRECTION OF DIFFRACTION ANGLE WITH INTERNAL STANDARD; 2.5.4 DETERMINATION OF FULL WIDTH AT HALF MAXIMUM INTENSITY; 2.5.5 ACCURACY OF THE VALUES DETERMINED; 2.6 DEGREE OF GRAPHITIZATION; 2.7 KEY ISSUES FOR MEASUREMENT; 2.7.1 DIFFRACTION PATTERN; 2.7.2 USE OF INTERNAL STANDARD; 2.7.3 USE OF THIN SAMPLE HOLDER; 2.7.4 INDEXING THE DIFFRACTION LINE; 2.7.5 SEPARATION INTO COMPONENT PROFILES; 2.8 CONCLUDING REMARKS; REFERENCES; 3
- Small-Angle X-ray Scattering.
- 3.1 INTRODUCTION3.2 FUNDAMENTALS; 3.3 KEY ISSUES FOR THE MEASUREMENTS; 3.4 APPLICATIONS FOR CARBON MATERIALS; 3.4.1 POROUS CARBON FIBERS; 3.4.2 GLASS-LIKE CARBONS; 3.4.3 MESOCELLULAR FOAM CARBONS (SILICA-TEMPLATED CARBONS); 3.4.4 OPEN PORES FORMED BY AIR OXIDATION; 3.5 CONCLUDING REMARKS; REFERENCES; 4
- Transmission Electron Microscopy; 4.1 INTRODUCTION; 4.2 MODES OF TRANSMISSION ELECTRON MICROSCOPY [3-5]; 4.2.1 DIFFRACTING MODE; 4.2.2 IMAGING MODES; 4.3 KEY ISSUES FOR OBSERVATION; 4.3.1 OBJECT THICKNESS (WEAK PHASE OBJECT) [6]
- 4.3.2 CONTRAST TRANSFER FUNCTION OF THE TRANSMISSION ELECTRON MICROSCOPE [6]4.3.2.1 Objective Lens Defects; 4.3.2.1.1 Spherical Aberration Cs; 4.3.2.1.1 Spherical Aberration Cs; 4.3.2.1.2 Objective Lens Aperture; 4.3.2.1.2 Objective Lens Aperture; 4.3.2.1.3 Ellipticity Astigmatism; 4.3.2.1.3 Ellipticity Astigmatism; 4.3.2.2 Illumination Defects; 4.3.2.2.1 Information Limit (Termination) [12]; 4.3.2.2.1 Information Limit (Termination) [12]; 4.3.2.2.2 Spatial Coherency; 4.3.2.2.2 Spatial Coherency; 4.3.3 DIFFUSION CONTRASTS; 4.3.4 FRESNEL FRINGES, IE, EDGE FRINGES [4]
- 4.5 APPLICATIONS FOR CARBON MATERIALS [1,2,5,17-19]4.5.1 TRANSMISSION ELECTRON MICROSCOPY MODES TO STUDY CRYSTALLINITY OF CARBON MATERIALS; 4.5.2 TRANSMISSION ELECTRON MICROSCOPY MODES IN THE STUDY OF CARBONIZATION AND GRAPHITIZATION; 4.6 CONCLUSIONS; REFERENCES; FURTHER READING; 5
- Scanning Electron Microscopy; 5.1 INTRODUCTION; 5.2 INSTRUMENTATION AND RESOLVING POWER; 5.2.1 INSTRUMENTATION; 5.2.2 MAGNIFICATION AND RESOLVING POWER OF THE SCANNING ELECTRON MICROSCOPE; 5.2.3 EDGE EFFECTS APPEARING IN SE MODE IMAGES; 5.3 SPECIMEN PREPARATION.