Gravimetric analysis Part III /
Gravimetric Analysis, Part III describes the experimental procedures for the gravimetric analysis of various compounds. This book is composed of 13 chapters that also present sample preparation protocols. The first four chapters survey the steps for halogen compound determination. The succeeding cha...
| Main Author: | Erdey, László, |
|---|---|
| Other Authors: | Svehla, G.,, Buzás, Ilona,, ScienceDirect (Online service) |
| Format: | eBook |
| Language: | English Hungarian |
| Published: |
Oxford :
Pergamon Press,
1965.
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| Physical Description: |
1 online resource. |
| Series: |
International series of monographs in analytical chemistry ;
Volume 7. |
| Subjects: |
| Summary: |
Gravimetric Analysis, Part III describes the experimental procedures for the gravimetric analysis of various compounds. This book is composed of 13 chapters that also present sample preparation protocols. The first four chapters survey the steps for halogen compound determination. The succeeding chapters provide the procedures for gravimetric determination of cyanide, thiocyanate ions, sulfur, nitrogen, phosphorus, carbon, silicon, and boron. The final chapter considers other aspects of gravimetric experiments, including apparatus cleaning, reagents, and numerical calculation of the result. Th. |
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| Item Description: |
Includes index. Front Cover; Gravimetric Analysis, Part III; Copyright Page; Table of Contents; CHAPTER 48. CHLORINE; 48.1. Digestion of organic halogen-containing substances; 48.2. Determination of chloride in the form of silver chloride; 48.3. Determination of perchlorate ions in the form of potassium perchlorate; 48.4-48.5. Separation Methods; References; CHAPTER 49. BROMINE; 49.1. Determination of bromide in the form of silver bromide; 49.2. Separation Methods; 49.3. INDIRECT DETERMINATION OF BROMIDE AND CHLORIDE; References; CHAPTER 50. IODINE; 50.1. Determination of iodide in the form of silver iodide. 50.2. Determination of iodide in the form of palladium(II) iodide50.3-50.5. Separation Methods; References; CHAPTER 51. FLUORINE; 51.1. Determination in the form of calcium fluoride; 51.2. Determination in the form of lead chlorofluoride; 51.3-51.5. Separation Methods; References; CHAPTER 52. CYANIDE; 52.1. Determination in the form of silver cyanide; 52.2. Determination of cyanide in mercury(II) cyanide; 52.3-52.4. Separation Methods; References; CHAPTER 53. THIOCYANATE IONS; 53.1. Determination in the form of silver thiocyanate; 53.2. Determination in the form of copper(I) thiocyanate. 53.3. Determination in the form of barium sulphate53.4-53.7. Separation Methods; References; CHAPTER 54. SULPHUR; 54.1. Determination of sulphate ions; 54.2. Determination of sulphide ions; 54.3. Determination of the sulphur content of non-volatile organic substances; 54.4. Determination of the sulphur content of volatile organic substances (petrol). Lamp sulphur; 54.5. Determination of the total sulphur content of gases; 54.6. Determination of the sulphur content of coal; 54.7. Digestion of organic substances containing sulphur with red fuming nitric acid in a bomb. 54.8. Determination of the sulphur content of non-volatile organic substances by combustion in a bomb (bomb sulphur)54.9. Determination of the sulphur content of organic substances after decomposition in a Parr bomb; 54.10. Determination of sulphite, dithionite, thiosulphate and peroxydisulphate ions; 54.11. Separation of sulphite and thiosulphate; 54.12. Simultaneous determination of sulphide, sulphite and thiosulphate; 54.13. Determination of elementary sulphur; References; CHAPTER 55. NITROGEN; 55.1. Determination in the form of nitron nitrate; References; CHAPTER 56. PHOSPHORUS. 56.1. Determination of phosphate ions56.2. Determination of pyrophosphate ions; 56.3. Determination of phosphite ions; 56.4. Determination of hypophosphite ions; 56.5. Determination of hypophosphate ions; 56.6-56.26. Separation of phosphorus compounds; References; CHAPTER 57. CARBON; 57.1. Determination of carbon and hydrogen in organic substances by combustion; 57.2. Determination of carbonates; 57.3. Determination of the carbon content of iron and steel; CHAPTER 58. SILICON; 58.1. Precipitation and dehydration of silicic acid; 58.2. Determination of the silicic acid content of silicates. Gravimetric Analysis, Part III describes the experimental procedures for the gravimetric analysis of various compounds. This book is composed of 13 chapters that also present sample preparation protocols. The first four chapters survey the steps for halogen compound determination. The succeeding chapters provide the procedures for gravimetric determination of cyanide, thiocyanate ions, sulfur, nitrogen, phosphorus, carbon, silicon, and boron. The final chapter considers other aspects of gravimetric experiments, including apparatus cleaning, reagents, and numerical calculation of the result. Th. |
| Physical Description: |
1 online resource. |
| ISBN: |
9781483222592 1483222594 |